Articles | Volume 7, issue 1
Solid Earth, 7, 129–140, 2016

Special issue: Pore-scale tomography & imaging - applications, techniques...

Solid Earth, 7, 129–140, 2016

Method article 26 Jan 2016

Method article | 26 Jan 2016

X-ray microtomography analysis of soil structure deformation caused by centrifugation

S. Schlüter1,2, F. Leuther1, S. Vogler2, and H.-J. Vogel1,3 S. Schlüter et al.
  • 1Department of Soil Physics, Helmholtz-Centre for Environmental Research – UFZ, Halle (Saale), Germany
  • 2German Center for Neurodegenerative Diseases (DZNE), Dresden, Germany
  • 3Soil Science, Martin-Luther-University Halle-Witteberg, Haale (Saale), Germany

Abstract. Centrifugation provides a fast method to measure soil water retention curves over a wide moisture range. However, deformation of soil structure may occur at high angular velocities in the centrifuge. The objective of this study was to capture these changes in soil structure with X-ray microtomography and to measure local deformations via digital volume correlation. Two samples were investigated that differ in texture and rock content. A detailed analysis of the pore space reveals an interplay between shrinkage due to drying and soil compaction due to compression. Macroporosity increases at moderate angular velocity because of crack formation due to moisture release. At higher angular velocities, corresponding to capillary pressure of ψ < −100 kPa, macroporosity decreases again because of structure deformation due to compression. While volume changes due to swelling clay minerals are immanent in any drying process, the compaction of soil is a specific drawback of the centrifugation method. A new protocol for digital volume correlation was developed to analyze the spatial heterogeneity of deformation. In both samples the displacement of soil constituents is highest in the top part of the sample and exhibits high lateral variability explained by the spatial distribution of macropores in the sample. Centrifugation should therefore only be applied after the completion of all other hydraulic or thermal experiments, or any other analysis that depends on the integrity of soil structure.

Short summary
A new protocol for digital volume correlation facilitates detailed insights into internal deformation of soil. Structure deformation during centrifugation is revealed by comparing X-ray CT images before and after centrifugation. Quantitative image analysis reveals that soil structure changes are driven by soil shrinkage due to drying and soil compaction due to compression.