Articles | Volume 12, issue 1
https://doi.org/10.5194/se-12-1-2021
© Author(s) 2021. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/se-12-1-2021
© Author(s) 2021. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
Research article
| 
11 Jan 2021
Research article |
| 11 Jan 2021
| 11 Jan 2021
Simulating permeability reduction by clay mineral nanopores in a tight sandstone by combining computer X-ray microtomography and focussed ion beam scanning electron microscopy imaging
Arne Jacob
CORRESPONDING AUTHOR
Geosciences Institute, Johannes Gutenberg-University, J.-J. Becherweg
21, 55099 Mainz, Germany
Markus Peltz
Institute of Geography and Geology, University Greifswald,
Friedrich-Ludwig-Jahn-Str. 17a, 17487 Greifswald, Germany
Sina Hale
Institute of Applied Geosciences (AGW), Karlsruhe Institute of
Technology (KIT), Kaiserstraße 12, 76131 Karlsruhe, Germany
Frieder Enzmann
Geosciences Institute, Johannes Gutenberg-University, J.-J. Becherweg
21, 55099 Mainz, Germany
Olga Moravcova
Geosciences Institute, Johannes Gutenberg-University, J.-J. Becherweg
21, 55099 Mainz, Germany
Laurence N. Warr
Institute of Geography and Geology, University Greifswald,
Friedrich-Ludwig-Jahn-Str. 17a, 17487 Greifswald, Germany
Georg Grathoff
Institute of Geography and Geology, University Greifswald,
Friedrich-Ludwig-Jahn-Str. 17a, 17487 Greifswald, Germany
Philipp Blum
Institute of Applied Geosciences (AGW), Karlsruhe Institute of
Technology (KIT), Kaiserstraße 12, 76131 Karlsruhe, Germany
Michael Kersten
Geosciences Institute, Johannes Gutenberg-University, J.-J. Becherweg
21, 55099 Mainz, Germany
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Cited
29 citations as recorded by crossref.
- Correct estimation of permeability using experiment and simulation S. Khirevich et al. https://doi.org/10.1063/5.0123673
- Multiscale pore network modeling and flow property analysis for tight sandstone: a case study X. Wu et al. https://doi.org/10.1093/jge/gxad092
- The alteration of illite by Bad Nauheim and Gerolstein brine; Implications on fluid permeability in geothermal systems E. Götz et al. https://doi.org/10.1016/j.clay.2023.107082
- A Correlative Approach for the Assessment of Porosity in Shale Rocks by Scanning Electron Microscopy F. Medina et al. https://doi.org/10.1093/mam/ozaf020
- Digital rock physics, chemistry, and biology: challenges and prospects of pore-scale modelling approach S. Sadeghnejad et al. https://doi.org/10.1016/j.apgeochem.2021.105028
- Efficient multi-scale image reconstruction of heterogeneous rocks with unresolved porosity using octree structures A. Moslemipour et al. https://doi.org/10.1007/s10596-025-10362-w
- MICP treated sand: insights into the impact of particle size on mechanical parameters and pore network after biocementation N. Erdmann et al. https://doi.org/10.1007/s43939-024-00108-3
- A Coupled Model for Upscaling Water Flow in a Shale Matrix System from Pore Scale to Representative Elementary Area Scale Y. Yang et al. https://doi.org/10.1021/acsomega.3c04817
- Pore Structure and Fractal Characteristics of Kelasu Ultra-Deep Tight Sandstone Gas Reservoirs L. Tang et al. https://doi.org/10.3390/pr13103074
- Digital core reconstruction research: challenges and prospects A. Ponomarev et al. https://doi.org/10.1080/24749508.2022.2086201
- Review of modern models of porous media for numerical simulation of fluid flows O. Simonov et al. https://doi.org/10.1016/j.heliyon.2023.e22292
- Fluid–Rock Interactions in Geothermal Reservoirs, Germany: Thermal Autoclave Experiments Using Sandstones and Natural Hydrothermal Brines R. Schäffer et al. https://doi.org/10.1007/s10498-022-09404-x
- Microscopic Conductivity Mechanism and Saturation Evaluation of Tight Sandstone Reservoirs: A Case Study from Bonan Oilfield, China J. Sun et al. https://doi.org/10.3390/en15041368
- Upscaling calcite dissolution rates in a tight reservoir sandstone S. Hale et al. https://doi.org/10.1007/s12665-022-10399-5
- Multi-physics evaluation of carbonate-rich source rocks from high-resolution images S. Eichmann et al. https://doi.org/10.1557/s43579-021-00113-0
- Image-Based Multi-scale Reconstruction of Unresolved Microporosity in 3D Heterogeneous Rock Digital Twins Using Cross-Correlation Simulation and Watershed Algorithm A. Moslemipour et al. https://doi.org/10.1007/s11242-024-02111-x
- Tight sandstone reservoirs in lacustrine environments: review and perspectives C. Hu et al. https://doi.org/10.1080/00206814.2025.2519039
- Minkowski functional evaluation of representative elementary volume of rock microtomography images at multiple resolutions S. Sadeghnejad et al. https://doi.org/10.1016/j.advwatres.2023.104501
- 3D-measurement of particles and particulate assemblies - A review of the paradigm shift in describing anisotropic particles X. Jia & R. Williams https://doi.org/10.1016/j.powtec.2024.120109
- Salt-induced structure damage and permeability enhancement of Three Gorges Reservoir sandstone under wetting-drying cycles X. Jiang et al. https://doi.org/10.1016/j.ijrmms.2022.105100
- Comparison of SEM-Assisted Nanoporometric and Microporometric Morphometric Techniques Applied for the Ultramicroporous Polymer Films I. Maklakova et al. https://doi.org/10.4028/www.scientific.net/KEM.899.660
- Developing synthetic sandstones using geopolymer binder for constraining coupled processes in porous rocks M. Peltz et al. https://doi.org/10.1007/s42452-023-05301-2
- Investigation of the Microscopic Pore–Throat Structure Difference of Tight Sandstone/Glutenite Based on a Multifractal Method Y. Chang et al. https://doi.org/10.1021/acs.energyfuels.3c00965
- The influence of spatial resolution and noise on fracture network properties calculated from X-ray microtomography data J. McBeck et al. https://doi.org/10.1016/j.ijrmms.2021.104922
- Characterizing pore structure and CO2 storage potential in Eocene Mirador Formation tight sandstones using X-ray micro-CT C. Ríos et al. https://doi.org/10.1016/j.jgsce.2025.205699
- Direct observation of fluid flow pattern formation in sandstone due to coupled dissolution and clogging processes J. Schabernack et al. https://doi.org/10.1016/j.jhydrol.2025.133868
- A FIB-SEM Study of Illite Morphology in Aeolian Rotliegend Sandstones: Implications for Understanding the Petrophysical Properties of Reservoir Rocks M. Peltz et al. https://doi.org/10.1007/s42860-022-00174-9
- Modeling of flow and transport in multiscale digital rocks aided by grid coarsening of microporous domains B. Shi et al. https://doi.org/10.1016/j.jhydrol.2024.131003
- Fractal analysis of CT images of tight sandstone with anisotropy and permeability prediction Y. Yang et al. https://doi.org/10.1016/j.petrol.2021.108919
29 citations as recorded by crossref.
- Correct estimation of permeability using experiment and simulation S. Khirevich et al. https://doi.org/10.1063/5.0123673
- Multiscale pore network modeling and flow property analysis for tight sandstone: a case study X. Wu et al. https://doi.org/10.1093/jge/gxad092
- The alteration of illite by Bad Nauheim and Gerolstein brine; Implications on fluid permeability in geothermal systems E. Götz et al. https://doi.org/10.1016/j.clay.2023.107082
- A Correlative Approach for the Assessment of Porosity in Shale Rocks by Scanning Electron Microscopy F. Medina et al. https://doi.org/10.1093/mam/ozaf020
- Digital rock physics, chemistry, and biology: challenges and prospects of pore-scale modelling approach S. Sadeghnejad et al. https://doi.org/10.1016/j.apgeochem.2021.105028
- Efficient multi-scale image reconstruction of heterogeneous rocks with unresolved porosity using octree structures A. Moslemipour et al. https://doi.org/10.1007/s10596-025-10362-w
- MICP treated sand: insights into the impact of particle size on mechanical parameters and pore network after biocementation N. Erdmann et al. https://doi.org/10.1007/s43939-024-00108-3
- A Coupled Model for Upscaling Water Flow in a Shale Matrix System from Pore Scale to Representative Elementary Area Scale Y. Yang et al. https://doi.org/10.1021/acsomega.3c04817
- Pore Structure and Fractal Characteristics of Kelasu Ultra-Deep Tight Sandstone Gas Reservoirs L. Tang et al. https://doi.org/10.3390/pr13103074
- Digital core reconstruction research: challenges and prospects A. Ponomarev et al. https://doi.org/10.1080/24749508.2022.2086201
- Review of modern models of porous media for numerical simulation of fluid flows O. Simonov et al. https://doi.org/10.1016/j.heliyon.2023.e22292
- Fluid–Rock Interactions in Geothermal Reservoirs, Germany: Thermal Autoclave Experiments Using Sandstones and Natural Hydrothermal Brines R. Schäffer et al. https://doi.org/10.1007/s10498-022-09404-x
- Microscopic Conductivity Mechanism and Saturation Evaluation of Tight Sandstone Reservoirs: A Case Study from Bonan Oilfield, China J. Sun et al. https://doi.org/10.3390/en15041368
- Upscaling calcite dissolution rates in a tight reservoir sandstone S. Hale et al. https://doi.org/10.1007/s12665-022-10399-5
- Multi-physics evaluation of carbonate-rich source rocks from high-resolution images S. Eichmann et al. https://doi.org/10.1557/s43579-021-00113-0
- Image-Based Multi-scale Reconstruction of Unresolved Microporosity in 3D Heterogeneous Rock Digital Twins Using Cross-Correlation Simulation and Watershed Algorithm A. Moslemipour et al. https://doi.org/10.1007/s11242-024-02111-x
- Tight sandstone reservoirs in lacustrine environments: review and perspectives C. Hu et al. https://doi.org/10.1080/00206814.2025.2519039
- Minkowski functional evaluation of representative elementary volume of rock microtomography images at multiple resolutions S. Sadeghnejad et al. https://doi.org/10.1016/j.advwatres.2023.104501
- 3D-measurement of particles and particulate assemblies - A review of the paradigm shift in describing anisotropic particles X. Jia & R. Williams https://doi.org/10.1016/j.powtec.2024.120109
- Salt-induced structure damage and permeability enhancement of Three Gorges Reservoir sandstone under wetting-drying cycles X. Jiang et al. https://doi.org/10.1016/j.ijrmms.2022.105100
- Comparison of SEM-Assisted Nanoporometric and Microporometric Morphometric Techniques Applied for the Ultramicroporous Polymer Films I. Maklakova et al. https://doi.org/10.4028/www.scientific.net/KEM.899.660
- Developing synthetic sandstones using geopolymer binder for constraining coupled processes in porous rocks M. Peltz et al. https://doi.org/10.1007/s42452-023-05301-2
- Investigation of the Microscopic Pore–Throat Structure Difference of Tight Sandstone/Glutenite Based on a Multifractal Method Y. Chang et al. https://doi.org/10.1021/acs.energyfuels.3c00965
- The influence of spatial resolution and noise on fracture network properties calculated from X-ray microtomography data J. McBeck et al. https://doi.org/10.1016/j.ijrmms.2021.104922
- Characterizing pore structure and CO2 storage potential in Eocene Mirador Formation tight sandstones using X-ray micro-CT C. Ríos et al. https://doi.org/10.1016/j.jgsce.2025.205699
- Direct observation of fluid flow pattern formation in sandstone due to coupled dissolution and clogging processes J. Schabernack et al. https://doi.org/10.1016/j.jhydrol.2025.133868
- A FIB-SEM Study of Illite Morphology in Aeolian Rotliegend Sandstones: Implications for Understanding the Petrophysical Properties of Reservoir Rocks M. Peltz et al. https://doi.org/10.1007/s42860-022-00174-9
- Modeling of flow and transport in multiscale digital rocks aided by grid coarsening of microporous domains B. Shi et al. https://doi.org/10.1016/j.jhydrol.2024.131003
- Fractal analysis of CT images of tight sandstone with anisotropy and permeability prediction Y. Yang et al. https://doi.org/10.1016/j.petrol.2021.108919
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Short summary
In this work, we combined different imaging and experimental measuring methods for analysis of cross-scale effects which reduce permeability of tight reservoir rocks. Simulated permeability of digital images of rocks is often overestimated, which is caused by non-resolvable clay content within the pores of a rock. By combining FIB-SEM with micro-XCT imaging, we were able to simulate the true clay mineral abundance to match experimentally measured permeability with simulated permeability.
In this work, we combined different imaging and experimental measuring methods for analysis of...
